Scanning Electron Microscopy: Difference between revisions

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For a video playlist with additional explanation of SEM operating procedures click [https://www.youtube.com/watch?v=F9jh7PNGqrw&list=PLuUTDbf8_YeL-z748VN6SejPdOToEacvE&index=2&t=0s here]-->
For a video playlist with additional explanation of SEM operating procedures click [https://www.youtube.com/watch?v=F9jh7PNGqrw&list=PLuUTDbf8_YeL-z748VN6SejPdOToEacvE&index=2&t=0s here]-->


[[Categories:Equipment]]
[[Category:Equipment]]

Revision as of 16:32, 31 May 2021

PhenomXL G2 SEM
Magnification Range: 360x to 190,000x
Feature Resolution: <500 nm
Detectors: Secondary (SED) & Backscatter (BSD)
Capabilities: EDS, automated image mapping
Sample Dimensions: <3cm tall, no magnetic samples
Phenom ProX SEM
Magnification Range: 40,000x to 100,000x
Feature Resolution: <500 nm
Detectors: Backscatter only
Capabilities: EDS
Sample Dimensions: <2.5cm in diameter, <3cm tall, no magnetic samples

A scanning electron microscope (SEM) uses an electron beam than scans across a sample, allowing for much higher magnifications compared to optical microscopy. The electrons are reflected off the sample (either elestically or ineleastically) and collected by a detector, yielding an image. The MILL currently owns two benchtop SEM systems: an older Phenom ProX and a new PhenomXL G2 (acquired May 2021). Both SEMs have backscattered electron detectors (BSD) for imaging and energy-dispersive X-ray spectroscopy (EDS) systems for elemental identification. The new PhenomXL contains an additional secondary electron detector (SED), which gives the images it captures better depth of field.

Theory

Electron Imaging

Detectors

EDS