X-ray Diffraction: Difference between revisions

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[[File:XRD.png|thumb|500px|Thermo Scientific ARL™ EQUINOX 100 X-ray diffractometer]]
[[File:XRD.png|thumb|500px|Thermo Scientific ARL™ EQUINOX 100 X-ray diffractometer]]
An '''X-ray diffractometer (XRD)''' detects crystalline phases in a sample by measuring the diffraction of X-rays at varying angles. For best results, samples should be ground into a fine powder so that the collective crystal has random orientations.
== Overview ==
An '''X-ray diffractometer (XRD)''' detects crystalline phases in a sample by measuring the diffraction pattern of X-rays at varying angles. X-rays are used because the interplanar spacing for the vast majority of crystalline materials falls in the range of X-ray wavelengths (0.01-10 nm). The MILL’s XRD is set up for powder X-ray diffraction: for the best results, samples should be ground into a fine powder so that the collective group of crystals has a random orientation.


== Operation ==
== Operation ==
This tool is not available for direct usage by users. Anyone who wishes to use or be trained on the XRD must undergo the general lab safety training '''AND''' the Georgia Tech Office of Radiological Safety (ORS) X-Ray Safety Training before reporting to the XRD Technical Officer.


The tool is not available for direct usage by users. Please visit Love 176 to fill out an XRD request slip and leave your sample in the XRD sample exchange box by the door. In order for your request to be processed, please email the team leader listed on the XRD request slip to notify them.
Otherwise, please visit Love 176 to fill out an XRD request slip and leave your sample in the XRD sample exchange box by the door. In order for your request to be processed, please email the technical officer listed on the XRD request slip to notify them.

Revision as of 18:26, 9 December 2020

File:XRD.png
Thermo Scientific ARL™ EQUINOX 100 X-ray diffractometer

Overview

An X-ray diffractometer (XRD) detects crystalline phases in a sample by measuring the diffraction pattern of X-rays at varying angles. X-rays are used because the interplanar spacing for the vast majority of crystalline materials falls in the range of X-ray wavelengths (0.01-10 nm). The MILL’s XRD is set up for powder X-ray diffraction: for the best results, samples should be ground into a fine powder so that the collective group of crystals has a random orientation.

Operation

This tool is not available for direct usage by users. Anyone who wishes to use or be trained on the XRD must undergo the general lab safety training AND the Georgia Tech Office of Radiological Safety (ORS) X-Ray Safety Training before reporting to the XRD Technical Officer.

Otherwise, please visit Love 176 to fill out an XRD request slip and leave your sample in the XRD sample exchange box by the door. In order for your request to be processed, please email the technical officer listed on the XRD request slip to notify them.