Thermogravimetric Analysis: Difference between revisions
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== Data Output & Analysis == | == Data Output & Analysis == | ||
TGA gives a mass vs. temperature plot. The absolute value of the derivative of mass vs. temperature is known as “DTG”, and can also be plotted against temperature. The degradation temperature of samples can be found from the largest value of DTG (point of fastest degradation). The 5%, 50%, and 99% mass lost temperatures (where applicable) can be determined from the initial mass. The primary component of initial weight loss is usually evaporation of moisture and other volatiles. At larger values of weight loss weight loss the primary factors are typically pyrolysis, reduction, and desorption. While both inert (<math> N_2 </math> or noble gas) and oxidizing (<math> O_2 </math>) atmospheres can be used for TGA, the inert atmosphere is often preferred so it doesn’t interact with the sample and cause unwanted weight gain, potentially ruining any data collected. | TGA gives a mass vs. temperature plot. The absolute value of the derivative of mass vs. temperature is known as “DTG”, and can also be plotted against temperature. The degradation temperature of samples can be found from the largest value of DTG (point of fastest degradation). The 5%, 50%, and 99% mass lost temperatures (where applicable) can be determined from the initial mass. The primary component of initial weight loss is usually evaporation of moisture and other volatiles. At larger values of weight loss weight loss the primary factors are typically pyrolysis, reduction, and desorption. While both inert (<math> N_2 </math> or noble gas) and oxidizing (<math> O_2 </math>) atmospheres can be used for TGA, the inert atmosphere is often preferred so it doesn’t interact with the sample and cause unwanted weight gain, potentially ruining any data collected. | ||
== References == | |||
<references /> | |||
[[Category:Equipment|meas]] | [[Category:Equipment|meas]] | ||
Revision as of 10:32, 25 June 2021
| TGA |
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| Projected availability: Fall 2021 |
Coming soon to the MILL!
Data Output & Analysis
TGA gives a mass vs. temperature plot. The absolute value of the derivative of mass vs. temperature is known as “DTG”, and can also be plotted against temperature. The degradation temperature of samples can be found from the largest value of DTG (point of fastest degradation). The 5%, 50%, and 99% mass lost temperatures (where applicable) can be determined from the initial mass. The primary component of initial weight loss is usually evaporation of moisture and other volatiles. At larger values of weight loss weight loss the primary factors are typically pyrolysis, reduction, and desorption. While both inert ([math]\displaystyle{ N_2 }[/math] or noble gas) and oxidizing ([math]\displaystyle{ O_2 }[/math]) atmospheres can be used for TGA, the inert atmosphere is often preferred so it doesn’t interact with the sample and cause unwanted weight gain, potentially ruining any data collected.